One-step synthesis of γ-Fe2O3/Fe3O4 nanocomposite for sensitive electrochemical detection of hydrogen peroxide

نویسندگان

چکیده

Maghemite/magnetite nanocomposite (γ-Fe2O3/Fe3O4) was prepared via an electrochemical method using pulse alternating current and applied for electrocatalytic reduction sensing of hydrogen peroxide. The structural compositional analysis the γ-Fe2O3/Fe3O4 characterized by XRD, SEM, TEM XPS. Its thermal decomposition behavior studied TG/DSC. mechanism formation proposed. Furthermore, H2O2 performance evaluated in 0.1 M KH2PO4. sensor exhibited a fast electron transfer process nanocomposite. optimized revealed remarkable low limit detection 0.05 μM, wide linear range from 0.0002 to 8 mM, response time 2 s. These results demonstrated that is promising efficient material H2O2.

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ژورنال

عنوان ژورنال: Electrochimica Acta

سال: 2021

ISSN: ['1873-3859', '0013-4686']

DOI: https://doi.org/10.1016/j.electacta.2021.137723